Potassium Perchlorate is usually made by double decomposition of KCl and Sodium Perchlorate. The Potassium Perchlorate is not very soluble and will ppt out immediately as a very fine crystalline product (your solution will look like yogurt if you add the KCl quickly) as soon as you add the KCl to the Sodium Perchlorate. If you are using Sodium Perchlorate solution from a cell there will be some Sodium Chlorate present in the electrolyte and it should be borne in mind that you will get some Chlorate contamination of your product. A Perchlorate product that is contaminated with Chlorate should be treated the same as if you had Chlorate when it comes to mixing with sulphur or other combustibles that are dangerous with Chlorate. If you want pure K Perchlorate you must destroy all of the Sodium Chlorate present in the Sodium Perchlorate by chemical means and then use the pure Sodium Perchlorate to make Potassium Perchlorate. You may be able to clean it up by recrystallization but it is a laborious task. You can check for the presence of Chlorate by using a sensitive test or use an excess of chemicals to by sure that all Chlorate is gone.
You can also make Potassium Perchlorate by decomposition of K Chlorate, it is quite a good way to make the stuff and AFSIK it will not be contaminated with K Chlorate so long as you heat to the correct temperature. The KCl (byproduct) will be fairly easy to get out of the Perchlorate.
Here is The Complete Guide to Fireworks Chemicals
If you want to start make it by tonight, Click and read The Complete Guide to Fireworks Chemicals Here.
Welcome to Cooking Chemicals!
This Ebook will take you through everything you need to know to build simple to advanced fireworks, as well as the chemicals you will need to make them!
IN FACT, YOU WILL LEARN TO MAKE CHEMICALS THAT CAN NOT EVEN BE SHIPPED!
No more 2lb per year limit on important chemicals!
Tired of having to risk you life by following the dangerous advice from online sources? Some of the guides out there are just plain dangerous! Finally, a source of accurate and safe instructions for all the chemicals you need for the most spectacular fireworks show!
This DIY guide was written for those without an in depth knowledge of chemistry or physics. It is now easier to follow, cheaper to build, and contains many more pictures!
800+ People are now using these methods from this Ebook!
Here's a sample of the projects you'll be confident in after reading this book The Complete Guide to Fireworks Chemicals Here.:
Making German Blackhead or bright Aluminum Powder in any mesh you want! ($1.60/lb)
Make fine and pure Potassium Nitrate ($1.15/lb)
Make Potassium Perchlorate and most other Chlorates and Perchlorates (for $1.50/lb)!
Make colored smoke bombs for paintball and more!
The Ninja Contact Smoke Bomb: A flash of light, a puff of smoke and you're gone!
Colored smoke bombs!
Homemade waterproof Visco and cannon fuse. (Pennies per foot)
HOW TO BLOW FIRE! -- Without putting gas in our mouth!
Thermite from scratch: Includes underwater thermite and grenade thermate!
Fundamental methods of black powder - a $30 Ebook with the best methods for black powder!
Top 15 Flash Powder Recipes. Perfect for fireworks, noise makers, movie effects and more!
Homemade rockets!!!
How to Make Copper Oxide for exploding Thermite!
How to Make Barium Nitrate (All green fireworks need this, but it can't be shipped!)
How to make Iron Oxide for Thermite!
How to make safe mini rockets with matches!
How to Make Sparklers: Different colors, shapes and sizes!
How to Make Strontium Nitrate: This alone with save you plenty in shipping!
Make stars for roman candles and shells!
Roman candles in any size!
Make your own dextrin for pennies!
Build a remote ignitor -- Never light a fuse again!
Homemade Nitric Acid and Sulfuric Acid (Save Hundreds with this chapter!)
Flash Paper and Flash Cotton for special effects, magic, and fireworks. ($0.15 per sheet)
30+ Page formula index -- make anything you would buy or see on the 4th of July!
Free Magic Tricks included -- Just because I think they are cool :-)
AND MUCH MORE!!
If you want to start make it by tonight, Click and read The Complete Guide to Fireworks Chemicals Here.
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2 comments:
This ebook is full of errors. It was a complete waste of my money. The advertisement is of far better quality than the actual book. I immediately complained:
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I am not happy with the quality of your ebook. The numerous mistakes and misspellings put me on guard and the obvious lack of technical chemical training makes the content downright dangerous.
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Here is his response:
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this book should never be used literally. It is a purely informational book and the fact that you were considering doing any of the things within the book is dangerous on your part. I am not trying to get angry but simply put things into perspective for you.
Sincerely
makechem
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I never said I was trying to do any of these things. I said the information is dangerous. It is. You were very wise not to put any actual passages from the book in your ad. If you did I don't think people would buy it. I consider you no better than a scam artist. Buyer beware!!
hello
first thank you for your best learns
second i cann't find the book (The Complete Guide to Fireworks Chemicals)
please send it to us or re up on a server that we can download it.
thank you alot
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